Dimethylformamide → HCID 61066807, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 5-bromo-2-chloro-pyridine (2.0 g), 1-butanethiol (1.3 mL), cesium carbonate (4.5 g) and DMF (5 mL) was heated to 60° C. for 3 hours. The mixture was diluted with water and extracted three times with EA. The combined organic phases were washed with brine, dried (Na2SO4) and concentrated to provide the subtitle compound. MS ESI+: m/z=246 [M+H]+.

Provenance & Evidence