HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86644151, compound → 2-Ethylpyridin-3-yl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86644151 | HCID 86644151 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Ethylpyridin-3-yl acetate | HCID 67121346 | 100% |
Reaction Steps
To a solution of 2-ethynylpyridin-3-yl acetate (5.0 g, 31 mmol) in ethanol (50 mL) was added PtO2 (0.50 g, 2.2 mmol). The mixture was degassed with nitrogen and placed under a double-layer balloon of hydrogen. The reaction was stirred at ambient temperature for 30 minutes. The mixture was filtered and concentrated in vacuo to give 2-ethylpyridin-3-yl acetate (5.1 g, 31 mmol) that was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853409B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-74b56711849d468d9e7f21fdbc87ce66 |
| Source note | uspto-grants-2014_10 |