HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 2-Methanesulfonyloxypentadecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Pentadecan-2-ol | HCID 96687 | — |
| Product | 2-Methanesulfonyloxypentadecane | HCID 15343308 | 95% |
Reaction Steps
The 2-methanesulfonyloxypentadecane was prepared from 2-pentadecanol (25 g, 109 mmol), methanesulfonylchloride (11.8 ml, 152 mmol) and diisopropylethylamine (22.8 ml, 131 mmol) as previously described in 95% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05620677 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-9f439c24b27e4f26bdd5ce7c4ae88d29 |
| Source note | uspto-grants-1997_04 |