Methylurea → HCID 131731933, compound

HRID 535212Notes

Reaction equation

[CH3:1][NH:2][C:3]([NH2:5])=[O:4].[S-:6][C:7]#[N:8].[Na+:9]>>[CH3:1][NH:2][C:3]([NH2:5])=[O:4].[S-:6][C:7]#[N:8].[Na+:9]

Participants

Reactant 2

HCID 11719Methylurea

HCID 516871Sodium thiocyanate

Product 1

HCID 131731933HCID 131731933, compoundYield 169.8%

Conditions

Temperature: 70 °C

Procedure

To a round-bottom flask, 4.5 g of purified methylurea and 2 g of NaSCN (sodium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 70° C. for 10 hours to obtain 6.5 g of methylurea-NaSCN eutectic mixture.

Sources & evidence

ORD record: ord-ea61e22701f6488b9ec60a75672cdfa6
Source dataset: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08858837B2

Reaction notes

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