Methyl Carbamate → HCID 131731935, compound

HRID 535214Notes

Reaction equation

[C:1](=[O:5])([O:3][CH3:4])[NH2:2].[S-:6][C:7]#[N:8].[Na+:9]>>[C:1](=[O:5])([O:3][CH3:4])[NH2:2].[S-:6][C:7]#[N:8].[Na+:9]

Participants

Reactant 2

HCID 11722Methyl Carbamate

HCID 516871Sodium thiocyanate

Product 1

HCID 131731935HCID 131731935, compoundYield 194.2%

Conditions

Temperature: 50 °C

Procedure

To a round-bottom flask, 13.7 g of purified methyl carbamate and 5 g of NaSCN (sodium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 50° C. for 50 minutes to obtain 18.7 g of methyl carbamate-NaSCN eutectic mixture.

Sources & evidence

ORD record: ord-f7d764affc4d4106900c220bf207b9eb
Source dataset: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08858837B2

Reaction notes

Loading…