HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → 2,2-Dimethyl-4,20-dioxo-3,9,12,15-tetraoxa-5,19-diazatricosan-23-oic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | Boc-TOTA | HCID 11989604 | — |
| Product | 2,2-Dimethyl-4,20-dioxo-3,9,12,15-tetraoxa-5,19-diazatricosan-23-oic acid | HCID 21881521 | — |
Reaction Steps
preparation from 1-(tert-butoxycarbonylamino)-4,7,10-trioxa-13-tridecanamine (5 g) and succinic anhydride (1.98) gave 7 g crude product. LCMS (Method 6): Rt 3.34 min; m/z (M+1) 421 Calcd: 421
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859493B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-bb636fe7fcda48309adf561c7eaad177 |
| Source note | uspto-grants-2014_10 |