(4-Chlorophenyl)acetic acid → HCID 70975926, compound

Participants

Reaction Steps

The product of Example 10B and 2-(4-chlorophenyl)acetic acid were treated using a method similar to that described in Example 10C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.73 (s, 1H), 8.40 (ddd, J=7.7, 1.6, 0.8 Hz, 1H), 8.17 (ddd, J=8.1, 1.3, 0.6 Hz, 1H), 8.04 (ddd, J=8.0, 7.2, 1.6 Hz, 1H), 7.98 (ddd, J=7.8, 7.2, 1.3 Hz, 1H), 7.81 (dd, J=5.1, 1.1 Hz, 1H), 7.65 (dd, J=3.6, 1.1 Hz, 1H), 7.35-7.47 (m, 4H), 7.28 (dd, J=5.1, 3.6 Hz, 1H), 3.72 (s, 2H); MS (APCI) M/Z 396 (M+H)+.

Provenance & Evidence