beta-Phenylisovaleric acid → HCID 71469283, compound

Participants

Reaction Steps

The product from Example 4B and 3-methyl-3-phenylbutanoic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.44 (s, 1H), 8.63-8.64 (m, 1H), 8.37-8.47 (m, 1H), 8.12 (dd, J=8.2, 2.5 Hz, 1H), 7.92-8.04 (m, 2H), 7.73-7.76 (m, 2H), 7.41-7.49 (m, 2H), 7.28-7.34 (m, 2H), 7.16-7.20 (m, 1H), 2.63 (s, 2H), 1.47 (s, 6H); MS (APCI) M/Z 433 (M+H)+.

Provenance & Evidence