3,5-Difluorophenylacetic acid → HCID 86673558, compound

Participants

Reaction Steps

The product from Example 30A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.66 (s, 1H), 8.42 (d, J=2.5 Hz, 1H), 8.33 (dd, J=7.9, 1.4 Hz, 1H), 8.06 (d, J=8.0 Hz, 1H), 7.95-8.00 (m, 1H), 7.87-7.93 (m, 1H), 7.74 (dd, J=8.2, 2.5 Hz, 1H), 7.45 (d, J=8.2 Hz, 1H), 7.05-7.21 (m, 3H), 4.39-4.40 (bs, 2H), 3.74 (s, 2H); MS (APCI) M/Z 441 (M+H)+.

Provenance & Evidence