(4-Chlorophenyl)acetic acid → HCID 86673560, compound

Participants

Reaction Steps

The product from Example 30A and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.60 (s, 1H), 8.42 (d, J=2.5 Hz, 1H), 8.32 (dd, J=7.9, 1.3 Hz, 1H), 8.06 (d, J=8.0 Hz, 1H), 7.97 (ddd, J=8.1, 7.2, 1.4 Hz, 1H), 7.90 (ddd, J=8.0, 7.2, 1.3 Hz, 1H), 7.73 (dd, J=8.2, 2.5 Hz, 1H), 7.46 (dd, J=8.2, 0.8 Hz, 1H), 7.39-7.43 (m, 2H), 7.35-7.38 (m, 2H), 4.39 (s, 2H), 3.68 (s, 2H); MS (APCI) M/Z 439 (M+H)+.

Provenance & Evidence