3-Amino-1-propanol → Dipyridodiazepinone deriv. 24

Participants

Reaction Steps

The title compound, m.p. 222°-224° C., was synthesized from 2-chloro-5,11-dihydro-11-ethyl-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 3-aminopropanol using procedures analogous to those described above, except that the mixture was heated in a pressure bottle at 210° C. for 40 min., and the product was crystallized from ethyl acetate.

Provenance & Evidence