3,5-Difluorophenylacetic acid → HCID 70976073, compound

Participants

Reaction Steps

The product from Example 57B and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound: 1H NMR (500 MHz, DMSO-d6) δ 11.74 (s, 1H), 8.35 (dd, J=7.9, 1.0, 1H), 8.09 (d, J=7.8, 1H), 8.04-7.98 (m, 1H), 7.94 (td, J=7.7, 1.1, 1H), 7.47-7.40 (m, 2H), 7.39-7.28 (m, 3H), 7.16 (tt, J=9.5, 2.3, 1H), 7.12-7.04 (m, 2H), 3.73 (s, 2H); MS (APCI+) M/Z 424 (M+H)+.

Provenance & Evidence