4-chlorophthalazin-1(2H)-one → HCID 70975938, compound

HRID 535531Notes

Reaction equation

HRID 535531 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5](=[O:12])[NH:4][N:3]=1.[SH:13][C:14]1[CH:19]=[CH:18][C:17]([NH:20][C:21](=[O:27])[O:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[CH:16][CH:15]=1>>[O:12]=[C:5]1[C:6]2[C:11](=[CH:10][CH:9]=[CH:8][CH:7]=2)[C:2]([S:13][C:14]2[CH:15]=[CH:16][C:17]([NH:20][C:21](=[O:27])[O:22][C:23]([CH3:25])([CH3:24])[CH3:26])=[CH:18][CH:19]=2)=[N:3][NH:4]1

Participants

3

Reactant 2

HCID 27751424-chlorophthalazin-1(2H)-oneHCID 59412418(4-Mercaptophenyl)carbamic acid tert-butyl ester

Product 1

HCID 70975938HCID 70975938, compound

Procedure

4-chlorophthalazin-1(2H)-one and tert-butyl 4-mercaptophenylcarbamate were processed using a method similar to that described in Example 57A to afford the title compound. MS (APCI+) M/Z 370 (M+H)+.

Sources & evidence

ORD record
ord-f6360daec2544832899a8b493e3703a9
Source dataset
uspto-grants-2014_10
Patent number
US08859549B2

Reaction notes

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