m-Tolylacetic acid → HCID 70976210, compound

Participants

Reaction Steps

The product of Example 1B and 2-(3-methylphenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/D2O) δ 8.31 (d, J=7.9, 1H), 8.04-8.01 (m, 1H), 8.01-7.96 (m, 1H), 7.94-7.88 (m, 1H), 7.26-7.22 (m, 1H), 7.19-7.16 (s, 2H), 7.11-7.08 (t, J=9.0, 1H), 3.86-3.78 (m, 4H), 3.62 (s, 2H), 3.13-3.06 (m, 4H), 2.31 (s, 3H); MS (ESI+) M/Z 379 (M+H)+.

Provenance & Evidence