p-Tolylacetic acid → HCID 70976227, compound

Participants

Reaction Steps

The product of Example 1B and 2-(4-methylphenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/D2O) δ 8.30 (dd, J=7.9, 0.8, 1H), 8.04-8.02 (m, 1H), 8.01-7.96 (m, 1H), 7.94-7.88 (m, 1H), 7.26 (d, J=8.0, 2H), 7.16 (d, J=7.9, 2H), 3.87-3.78 (m, 4H), 3.61 (s, 2H), 3.13-3.05 (m, 4H), 2.30 (s, 3H); MS (ESI+) M/Z 379 (M+H)+.

Provenance & Evidence