2-Methoxyphenylacetic acid → HCID 70975929, compound

Participants

Reaction Steps

The product of Example 1B and 2-(2-methoxyphenyl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.32 (dd, J=7.9, 1.3 Hz, 1H), 8.03 (d, J=8.0 Hz, 1H), 7.97-8.01 (m, 1H), 7.91 (td, J=7.5, 1.3 Hz, 1H), 7.33 (dd, J=7.4, 1.7 Hz, 1H), 7.27 (td, J=7.8, 1.7 Hz, 1H), 7.00 (d, J=8.7 Hz, 1H), 6.93 (td, J=7.4, 1.1 Hz, 1H), 3.85-3.82 (m, 4H), 3.82 (s, 3H), 3.62 (s, 2H), 3.09-3.11 (m, 4H); MS (ESI+) M/Z 395 (M+H)+.

Provenance & Evidence