HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Benzyloxyphenylacetic acid → HCID 70976151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Benzyloxyphenylacetic acid | HCID 81033 | — |
| Reactant | 2-amino-4-morpholinophthalazin-1(2H)-one | HCID 70976104 | — |
| Product | HCID 70976151 | HCID 70976151 | — |
Reaction Steps
The product of Example 1B and 2-[4-(benzyloxy)phenyl]acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.30 (dd, J=7.9, 1.2 Hz, 1H), 8.02 (d, J=1.2 Hz, 1H), 7.97-8.00 (m, 1H), 7.89-7.92 (m, 1H), 7.28-7.47 (m, 7H), 6.98-7.00 (m, 2H), 5.10 (s, 2H), 3.75-3.83 (m, 4H), 3.58-3.60 (m, 2H), 3.07-3.13 (m, 4H); MS (ESI−) M/Z 469 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-54e0992702274c8285b67a77bac041ef |
| Source note | uspto-grants-2014_10 |