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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 535585Generated: October 30, 2026

4-Benzyloxyphenylacetic acid → HCID 70976151, compound

https://huagongshe.com/reaction/535585

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Benzyloxyphenylacetic acidHCID 81033—
Reactant2-amino-4-morpholinophthalazin-1(2H)-oneHCID 70976104—
ProductHCID 70976151HCID 70976151—

Reaction Steps

The product of Example 1B and 2-[4-(benzyloxy)phenyl]acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.30 (dd, J=7.9, 1.2 Hz, 1H), 8.02 (d, J=1.2 Hz, 1H), 7.97-8.00 (m, 1H), 7.89-7.92 (m, 1H), 7.28-7.47 (m, 7H), 6.98-7.00 (m, 2H), 5.10 (s, 2H), 3.75-3.83 (m, 4H), 3.58-3.60 (m, 2H), 3.07-3.13 (m, 4H); MS (ESI−) M/Z 469 (M−H)−.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08859549B2
Source datasetuspto-grants-2014_10
ORD IDord-54e0992702274c8285b67a77bac041ef
Source noteuspto-grants-2014_10