HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaleneacetic Acid → HCID 70975816, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaleneacetic Acid | HCID 6862 | — |
| Reactant | 2-amino-4-morpholinophthalazin-1(2H)-one | HCID 70976104 | — |
| Product | HCID 70975816 | HCID 70975816 | — |
Reaction Steps
The product of Example 1B and 2-(naphthalen-1-yl)acetic acid were treated using a method similar to that described in Example 111 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.31 (dd, J=7.9, 1.3 Hz, 1H), 8.18 (d, J=8.2 Hz, 1H), 7.87-8.04 (m, 5H), 7.49-7.62 (m, 4H), 4.15 (s, 2H), 3.78-3.85 (m, 4H), 3.07-3.12 (m, 4H); MS (ESI−) M/Z 413 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859549B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-045a44ae045c4f5294834522490d8ba7 |
| Source note | uspto-grants-2014_10 |