Cyclopentyl chloroformate → HCID 123267304, compound

Participants

Reaction Steps

The product of Example 42 and cyclopentyl carbonochloridate were treated using a method similar to that described in Example 128 to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.60-11.62 (bs, 1H), 8.32 (d, J=7.8 Hz, 1H), 8.10 (d, J=8.0 Hz, 1H), 7.88-8.03 (m, 2H), 7.58-7.64 (m, 1H), 7.23-7.45 (m, 4H), 4.95-5.01 (bs, 1H), 4.47-4.50 (m, 2H), 3.67-3.68 (bs, 2H), 1.76-1.81 (m, 2H), 1.50-1.69 (m, 6H); MS (ESI+) M/Z 455 (M+H)+.

Provenance & Evidence