Benzyl chloroformate → HCID 123534900, compound

Participants

Reaction Steps

The product of Example 42 and benzyl carbonochloridate were treated using a method similar to that described in Example 128 to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.50-11.71 (m, 1H), 8.32 (dd, J=7.6, 1.5 Hz, 1H), 8.08-8.11 (m, 1H), 7.88-8.01 (m, 3H), 7.28-7.48 (m, 9H), 5.06-5.07 (bs, 2H), 4.54 (d, J=5.9 Hz, 2H), 3.68 (s, 2H); MS (ESI+) M/Z 494 (M+NH4)+.

Provenance & Evidence