4-chlorophthalazin-1(2H)-one → HCID 70975936, compound

HRID 535606Notes

Reaction equation

HRID 535606 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5](=[O:12])[NH:4][N:3]=1.[N:13]1[CH:18]=[CH:17][C:16]([SH:19])=[CH:15][CH:14]=1>>[N:13]1[CH:18]=[CH:17][C:16]([S:19][C:2]2[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5](=[O:12])[NH:4][N:3]=2)=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 27751424-chlorophthalazin-1(2H)-oneHCID 178418431pyridine-4-thiol

Product 1

HCID 70975936HCID 70975936, compound

Procedure

4-chlorophthalazin-1(2H)-one and pyridine-4-thiol were processed using a method similar to that described in Example 57A to afford the title compound. MS (APCI) M/Z 256 (M+H)+.

Sources & evidence

ORD record
ord-3633ffe4399042fbb8cc78a65b3e3791
Source dataset
uspto-grants-2014_10
Patent number
US08859549B2

Reaction notes

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