beta-Phenylisovaleric acid → HCID 70976040, compound

Participants

Reaction Steps

The product from Example 68B and 3-methyl-3-phenylbutanoic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ 11.45 (s, 1H), 8.56 (d, J=8.2, 1H), 8.41-8.34 (m, 1H), 8.14-8.08 (m, 1H), 8.04-7.96 (m, 3H), 7.84-7.77 (m, 1H), 7.68 (dd, J=10.8, 5.0, 2H), 7.38 (dd, J=8.4, 1.1, 2H), 7.33-7.27 (m, 2H), 7.20-7.14 (m, 1H), 2.54 (s, 2H), 1.32 (s, 6H); MS (DCI+) M/Z 479 (M+NH4)+.

Provenance & Evidence