4-Bromothiophenol → HCID 70975952, compound

HRID 535611Notes

Reaction equation

HRID 535611 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5](=[O:12])[NH:4][N:3]=1.[Br:13][C:14]1[CH:19]=[CH:18][C:17]([SH:20])=[CH:16][CH:15]=1>>[Br:13][C:14]1[CH:19]=[CH:18][C:17]([S:20][C:2]2[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5](=[O:12])[NH:4][N:3]=2)=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 660494-BromothiophenolHCID 27751424-chlorophthalazin-1(2H)-one

Product 1

HCID 70975952HCID 70975952, compound

Procedure

4-chlorophthalazin-1(2H)-one and 4-bromobenzenethiol were processed using a method similar to that described in Example 57A to afford the title compound. MS (APCI) M/Z 374 (M+CH3CN)+.

Sources & evidence

ORD record
ord-685913f5f9084cfeb07c4aeb3aa1f802
Source dataset
uspto-grants-2014_10
Patent number
US08859549B2

Reaction notes

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