3,5-Difluorophenylacetic acid → HCID 70976245, compound

Participants

Reaction Steps

The product from Example 195B and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ 11.76 (s, 1H), 8.39-8.32 (m, 1H), 8.08-8.04 (m, 1H), 8.02 (ddd, J=8.1, 7.6, 1.3, 1H), 7.95 (td, J=8.2, 1.3, 1H), 7.59-7.52 (m, 2H), 7.38 (ddd, J=6.6, 2.4, 1.4, 2H), 7.19-7.13 (m, 1H), 7.12-7.05 (m, 2H), 3.73 (s, 2H); MS (DCI+) M/Z 502 (M+H)+.

Provenance & Evidence