Benzeneacetic acid, 4-bromo- → HCID 70975928, compound

Participants

Reaction Steps

The product from Example 68B and 2-(4-bromophenyl)acetic acid were processed using a method similar to that described in Example 10C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ 11.86 (s, 1H), 8.56 (d, J=8.1, 1H), 8.38 (dd, J=8.0, 0.9, 1H), 8.14-8.08 (m, 1H), 8.01 (ddd, J=7.3, 4.4, 1.2, 3H), 7.80 (ddd, J=7.0, 4.0, 1.2, 1H), 7.68 (dd, J=10.6, 5.0, 2H), 7.58-7.51 (m, 2H), 7.25 (d, J=8.4, 2H), 3.66 (s, 2H); MS (ESI+) M/Z 498 (M+H)+, 515 (M+NH4)+, 556 (M+CH3CN+NH4)+.

Provenance & Evidence