HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → 4-(3-Acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | Cni H1594 | HCID 133110 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 4-(3-Acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide | HCID 12093259 | — |
Reaktionsschritte
Compound No. 14: 4-(3-acetylphenyl)amino-2-amino-6-methylpyrimidine, Compound No. 15, (0.968 g) was suspended in acetone (5 mL) containing methyl iodide (2 mL) was heated at reflux for 48 hr. Filtration after cooling gave 0.657 g of 4-(3-acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide as a white powder, mp 238°-40° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05620983 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-a241814cf0994d4d9216e4cdc728b2c5 |
| Quellennotiz | uspto-grants-1997_04 |