HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → 2-(4,5-dihydro-1H-imidazol-2-yl)-5-methoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2-Amino-4-methoxybenzonitrile | HCID 3723128 | — |
| Product | 2-(4,5-dihydro-1H-imidazol-2-yl)-5-methoxyaniline | HCID 58377389 | — |
Reaction Steps
The procedure used for the preparation of Intermediate C, Step 3 was used to prepare the title compound from 2-amino-4-methoxybenzonitrile (Step 1) and ethylene diamine. High vacuum drying gave the title compound (44 g, 92%). HPLC MS RT=1.04 min, MH+=192.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08859572B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-6f1f7ea4199742c8a19fd19163199517 |
| Source note | uspto-grants-2014_10 |