化工社化工社 化学情報印刷レポート · 研究参考用
tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate → tert-Butyl 4-(3-benzyloxyphenyl)-4-hydroxy-3-methylpiperidine-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate | HCID 22644642 | — |
| 反応物 | HCID 178419633 | HCID 178419633 | — |
| 生成物 | tert-Butyl 4-(3-benzyloxyphenyl)-4-hydroxy-3-methylpiperidine-1-carboxylate | HCID 86676855 | 44% |
反応手順
This compound was prepared from tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate and 3-benzyloxyphenylmagnesium bromide as described in Step 1 of Example 6 in 44% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08859777B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-0fbfab2e44194e98ae04264082fcc295 |
| 出典メモ | uspto-grants-2014_10 |