p-Fluoronitrobenzene → HCID 68156742, compound

HRID 537445Notes

Reaction equation

HRID 537445 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[F:11][C:12]([F:19])([F:18])[C:13]1[CH:14]=[N:15][NH:16][CH:17]=1>>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([N:15]2[CH:14]=[C:13]([C:12]([F:19])([F:18])[F:11])[CH:17]=[N:16]2)=[CH:3][CH:4]=1)([O-:10])=[O:9]

Participants

3

Reactant 2

HCID 9590p-FluoronitrobenzeneHCID 127777954-(Trifluoromethyl)-1H-pyrazole

Product 1

HCID 68156742HCID 68156742, compound

Procedure

The title compound was prepared by a method analogous to that described for Intermediate (3), using 1-fluoro-4-nitrobenzene and 4-(trifluoromethyl)-1H-pyrazole. 1H NMR (400 MHz, CDCl3, δ): 8.38 (m, 1H), 8.30 (m, 1H), 7.97 (s, 2H), 7.90 (m, 2H).

Sources & evidence

ORD record
ord-2410983b8cbe4eb0925f4bd43e042ba3
Source dataset
uspto-grants-2014_10
Patent number
US08859591B2

Reaction notes

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