HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 46312742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 4-Fluorophenylboronic acid | HCID 285645 | — |
| Reactant | 5-Bromo-2-fluoropyridine | HCID 2783168 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 46312742 | HCID 46312742 | 84.2% |
Reaction Steps
The procedure described in Example 4, step 4.2 is followed. Starting from 2.0 g (14.29 mmol) of 4-fluorobenzeneboronic acid, 5.21 g (14.29 mmol) of 5-bromo-2-fluoropyridine, 0.82 g (0.71 mmol) of Pd(PPh3)4 and 50 ml of a 1M aqueous solution of sodium carbonate, 2.30 g of product is obtained in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08865738B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-c58c7cba28de4b538a21ef0473839bc9 |
| Source note | uspto-grants-2014_10 |