Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3(2H,4H)-isoquinolinedione → 2-Methyl-4-(3'-oxo-4'-phenylthiobutyl)-homophthalimide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3(2H,4H)-isoquinolinedione | HCID 349435 | — |
| 반응물 | 3-Buten-2-one, 1-(phenylthio)- | HCID 10943029 | — |
| 반응물 | 3(2H)-Phenanthridinone | HCID 19960948 | — |
| 반응물 | 2-Methyl-homophthalimide | HCID 131719975 | — |
| 생성물 | 2-Methyl-4-(3'-oxo-4'-phenylthiobutyl)-homophthalimide | HCID 131719974 | — |
반응 단계
3(2H)-Phenanthridinone derivatives have been prepared from homophthalimide by the method of H. Iida et al., (Heterocycles 1983, 20, 227-30). 2-Methyl-homophthalimide is reacted with phenylthiomethyl vinyl ketone (prepared by the method A. G. Schultz et al.,J. Am. Chem. Soc. 1978, 100, 2140-9) in the presence of Triton B according to the described method to form 2-methyl-4-(3'-oxo-4'-phenylthiobutyl)-homophthalimide 9.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05621104 |
| 출처 데이터셋 | uspto-grants-1997_04 |
| ORD ID | ord-684e4f810aba4db194a155840fddfdc1 |
| 출처 메모 | uspto-grants-1997_04 |