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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 538821Generated: October 28, 2026

Iodine → HCID 66851637, compound

https://huagongshe.com/reaction/538821

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIodineHCID 807—
ReactantIsobutylamineHCID 6558—
ReactantTetrahydro-4H-pyran-4-oneHCID 121599—
ReactantPotassium thiocyanateHCID 516872—
ProductHCID 66851637HCID 66851637—

Reaction Steps

Commercially available dihydro-2H-pyran-4(3H)-one (Aldrich), 2-methylpropan-1-amine (Aldrich), potassium thiocyanate (Aldrich) and iodine (EMD chemicals) were processed using the method described in Example 91A to afford the title compound. MS (ESI+) m/z 213 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08865753B2
Source datasetuspto-grants-2014_10
ORD IDord-298fa34b6cab4b4f9f96b94a4a4be8a0
Source noteuspto-grants-2014_10