3-Bromo-2-methyl-1-propene → HCID 86694365, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described for step 23.7 from (S)-benzyl 4-methoxybenzyl(1-oxopropan-2-yl)carbamate and 3-bromo-2-methylprop-1-ene to afford the title compound as a 3:1 mixture of (2S,3R)- and (2S,3S)-diastereomer: tR=1.322 min (major isomer) and 1.329 min (minor isomer) (UPLC 1); tR=1.23 min (major isomer) and 1.24 min (minor isomer) (LC-MS 3); ESI-MS: 384 [M+H]+ (LC-MS 3).

Provenance & Evidence