HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 86629950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 2-(Isopropyl)-5-methylcyclohexylamine | HCID 89497 | — |
| Product | HCID 86629950 | HCID 86629950 | — |
Reaction Steps
The aforementioned product is obtained as a colorless solid containing in total 97.6% of the desired neomenthylamine derivatives from racemic neomenthylamine, as in the GP, by reaction with benzoylchloride. Furthermore, two further isomeric menthylamine derivatives are present at 1.3% and 1.0%, corresponding to a purity of isomeric N-(-2-isopropyl-5-methylcyclohexyl)benzamides of 99.9%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871288B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-d4e23fa94d804d059430b2cce77fc5f3 |
| Source note | uspto-grants-2014_10 |