HuagongsheHuagongshe Chemistry Print Report · For research reference only
Veratroyl chloride → HCID 86629951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Veratroyl chloride | HCID 77070 | — |
| Reactant | Cyclohexanamine, 5-methyl-2-(1-methylethyl)- | HCID 89497 | — |
| Product | HCID 86629951 | HCID 86629951 | — |
Reaction Steps
The aforementioned product is obtained as a colorless solid containing in total 97.8% of the desired neomenthylamine derivatives from racemic neomenthylamine, as in the GP, by reaction with 3,4-dimethoxybenzoylchloride. Furthermore, two further isomeric menthylamine derivatives are present at 1.3% and 0.9%, corresponding to a purity over all stereoisomers of 100.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871288B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-35c8567deb714321bb7fc5e9cbb0f60c |
| Source note | uspto-grants-2014_10 |