HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanamine, 5-methyl-2-(1-methylethyl)- → HCID 86629952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanamine, 5-methyl-2-(1-methylethyl)- | HCID 89497 | — |
| Reactant | (3,4-Dimethoxyphenyl)acetyl chloride | HCID 3604458 | — |
| Product | HCID 86629952 | HCID 86629952 | — |
Reaction Steps
The aforementioned product is obtained as a colorless solid containing in total 94.2% of the desired neomenthylamine derivatives from racemic neomenthylamine, as in the GP, by reaction with (3,4-dimethoxyphenyl)acetyl chloride. Furthermore, two further isomeric menthylamine derivatives are present at 2.7% and 2.5%, corresponding to a purity over all stereoisomers of 99.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871288B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-a194433508cd411f83af680d51d55d99 |
| Source note | uspto-grants-2014_10 |