HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 3,4,5-trimethoxy- → HCID 86629953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 3,4,5-trimethoxy- | HCID 78282 | — |
| Reactant | 2-(Isopropyl)-5-methylcyclohexylamine | HCID 89497 | — |
| Product | HCID 86629953 | HCID 86629953 | — |
Reaction Steps
The aforementioned product is obtained as a colorless solid containing in total 92.2% of the desired neomenthylamine derivatives from racemic neomenthylamine, as in the GP, by reaction with 3,4,5-trimethoxybenzoylchloride. Furthermore, two further isomeric menthylamine derivatives are present at 3.8% and 4.0%, corresponding to a purity over all stereoisomers of 100.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871288B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-d0063010c92f41b481cb5cc99209e7b9 |
| Source note | uspto-grants-2014_10 |