HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 2-Azidopropyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 3-Azidopropan-1-ol | HCID 10996974 | — |
| Reactant | 2-Azidoethyl methanesulfonate | HCID 11275197 | — |
| Product | 2-Azidopropyl methanesulfonate | HCID 89306959 | — |
Reaction Steps
Reaction of 3-azidopropanol (1.00 g, 9.90 mmol) and mesyl chloride (1.14 mL, 14.85 mmol) within 3 h as described for synthesis of 156a gave compound 156b (1.18 g) as a crude colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871728B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-38b5f3443f294edeb1f91eef8afdbc03 |
| Source note | uspto-grants-2014_10 |