HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanesulfonyl chloride → 2-Azidobutyl methanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Edukt | 2-Azidoethyl methanesulfonate | HCID 11275197 | — |
| Edukt | 4-AZIDOBUTAN-1-OL | HCID 12202790 | — |
| Produkt | 2-Azidobutyl methanesulfonate | HCID 86675084 | — |
Reaktionsschritte
Reaction of 4-azidobutanol (0.80 g, 6.95 mmol) and mesyl chloride (1.48 mL, 10.43 mmol) within 3 h as described for synthesis of 156a gave compound 156c (1.33 g) as a crude colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08871728B2 |
| Quelldatensatz | uspto-grants-2014_10 |
| ORD ID | ord-45285be625b4426283ae0b218e93bca0 |
| Quellennotiz | uspto-grants-2014_10 |