HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → [2,4'-Bipyridine]-3-carboxylic acid dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl [2,4'-bipyridine]-3-carboxylate | HCID 46317743 | — |
| Product | [2,4'-Bipyridine]-3-carboxylic acid dihydrochloride | HCID 84819756 | — |
Reaction Steps
A solution of ethyl 2,4′-bipyridine-3-carboxylate (14.1 g) in 6 N hydrochloric acid (200 mL) was heated under reflux overnight. The solvent was evaporated under reduced pressure, to the obtained residue was added toluene, and the solvent was again evaporated under reduced pressure to give the title compound (16.4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871766B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-af342559611d457797a69a3465b00847 |
| Source note | uspto-grants-2014_10 |