反应详情

A suspension of 1-(methylsulfanyl)-4-nitrobenzene (10.5 g, 0.062 mol) and Raney nickel (5 g) in methanol (250 ml) was hydrogenated in a round flask equipped with a balloon filled with hydrogen at room temperature for 16 hours. The resulting mixture was filtered and concentrated in vacuo to afford 8.0 g of 4-(methylsulfanyl)aniline as colorless oil.

1. customwas hydrogenated in a round flask
2. customequipped with a balloon
3. filtrationThe resulting mixture was filtered
4. concentrationconcentrated in vacuo