Cyclopropanemethanol → HCID 67151284, compound

HRID 541100Notes

Reaction equation

HRID 541100 reaction equation
[CH3:1][C:2]([CH2:8][CH2:9][CH3:10])=[CH:3][C:4]([O:6][CH3:7])=[O:5].[CH:11]1(CO)[CH2:13][CH2:12]1>>[CH3:1][C:2]([CH2:8][CH2:9][CH3:10])=[CH:3][C:4]([O:6][CH2:7][CH:11]1[CH2:13][CH2:12]1)=[O:5]

Participants

3

Reactant 2

HCID 75644CyclopropanemethanolHCID 574152Methyl 3-methyl-2-hexenoate

Product 1

HCID 67151284HCID 67151284, compound

Procedure

Prepared from methyl 3-methylhex-2-enoate and cyclopropanemethanol according to the ester preparation method B described above. The Z and E isomer were separated by distillation under vacuum using a 35 cm Fischer Spaltrohr® column.

Workup

  1. customThe Z and E isomer were separated by distillation under vacuum

Sources & evidence

ORD record
ord-903d899ebf9245189f71887e9460dd04
Source dataset
uspto-grants-2014_10
Patent number
US08871967B2

Reaction notes

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