HCID 68288627, compound → HCID 86672526, compound

HRID 541236Notes

Reaction equation

HRID 541236 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH:9]2[CH:11]([C:12]([OH:14])=O)[CH:10]2[C:15]([OH:17])=[O:16])=[CH:5][CH:4]=1>CC(OC(C)=O)=O>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH:9]2[CH:10]3[CH:11]2[C:12](=[O:14])[O:17][C:15]3=[O:16])=[CH:7][CH:8]=1

Participants

3

Reactant 1

HCID 68288627HCID 68288627, compound

Product 1

HCID 86672526HCID 86672526, compound

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Procedure

A mixture of 3-(4-methoxyphenyl)cyclopropane-1,2-dicarboxylic acid (crude product from the previous step) in Ac2O (20 mL) was heated under reflux for 1 h. Excess Ac2O was removed under reduced pressure. The crude product was used in the next step without further purification.

Workup

  1. temperaturewas heated
  2. temperatureunder reflux for 1 h
  3. customExcess Ac2O was removed under reduced pressure
  4. customThe crude product was used in the next step without further purification

Sources & evidence

ORD record
ord-e63f194b487b40088fa8b6018e9c2dae
Source dataset
uspto-grants-2014_10
Patent number
US08871790B2

Reaction notes

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