HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-bromo-2-methylbenzoate → Methyl 4-(cyclobutylmethyl)-2-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-bromo-2-methylbenzoate | HCID 22031226 | — |
| Reactant | Methyl 4-cyclobutyl-2-ethylbenzoate | HCID 68288811 | — |
| Reactant | HCID 178419648 | HCID 178419648 | — |
| Reactant | HCID 178419658 | HCID 178419658 | — |
| Product | Methyl 4-(cyclobutylmethyl)-2-methylbenzoate | HCID 68288684 | 84% |
Reaction Steps
The title compound (4.00 g, yellow oil, 84%) was prepared using a procedure similar to that used for the preparation of compound 181.3 using compound 152.1 (5.00 g) and cyclobutylmethylmagnesium bromide in place of compound 181.2 and cyclobutylmagnesium bromide respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871790B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-510d1ff8af134801b5152adace4e4b79 |
| Source note | uspto-grants-2014_10 |