Acetyl chloride → HCID 69016086, compound

Participants

Reaction Steps

The desired compound was prepared according to the procedure of Example A20, using N-[6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20), 3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]piperidine-3-carboxamide bis(trifluoroacetate) and acetyl chloride as starting materials in 34% yield. LCMS for C26H28ClN6O2 (M+H)+: m/z=491.2.

Provenance & Evidence