HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 66897812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 86636140 | HCID 86636140 | — |
| Product | HCID 66897812 | HCID 66897812 | 40% |
Reaction Steps
The desired compound was prepared according to the procedure of Example A9, step H using (3R)—N-[6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]pyrrolidine-3-carboxamide bis(trifluoroacetate) and isocyanato-ethane as starting materials in 40% yield. LCMS for C26H29ClN7O2 (M+H)+: m/z=506.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-8084d395263543af8b4edca54fa346cc |
| Source note | uspto-grants-2014_10 |