HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 69014435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 86636141 | HCID 86636141 | — |
| Product | HCID 69014435 | HCID 69014435 | 58% |
Reaction Steps
The desired compound was prepared according to the procedure of Example A20, using N-[6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20), 3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]-2-piperidin-4-ylacetamide bis(trifluoroacetate) and benzoyl chloride as starting materials in 58% yield. LCMS for C32H32ClN6O2 (M+H)+: m/z=567.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-6e1868b391704a33bb49fff8b89aaff4 |
| Source note | uspto-grants-2014_10 |