HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 69015051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | HCID 86636144 | HCID 86636144 | — |
| Product | HCID 69015051 | HCID 69015051 | 35% |
Reaction Steps
The desired compound was prepared according to the procedure of Example A9, step H using 3-amino-N-[6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]propanamide bis(trifluoroacetate) and phenyl isocyanate as starting materials in 35% yield. LCMS for C28H27ClN7O2 (M+H)+: m/z=528.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-17e4989b3abd4faa9aa9339a7f258935 |
| Source note | uspto-grants-2014_10 |