HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanesulfonyl chloride → HCID 69016455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | HCID 86636141 | HCID 86636141 | — |
| Product | HCID 69016455 | HCID 69016455 | 27% |
Reaction Steps
The desired compound was prepared according to the procedure of Example A42, using N-[6-chloro-2,4,8,22-tetraazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]-2-piperidin-4-ylacetamide bis(trifluoroacetate) and propane-2-sulfonyl chloride as starting materials in 27% yield. LCMS for C28H34ClN6O3S (M+H)+: m/z=569.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08871753B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-68b62bea31574e3eb6c51e8f84bf5c85 |
| Source note | uspto-grants-2014_10 |