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HRID541752

反应详情

EQUATION

反应方程式

HRID 541752 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)Nc1ccc([N+](=O)[O-])cc1I
HCID7098713

tert-butyl 4-nitro-2-iodophenylcarbamate

C11H13IN2O4

结构：C#Cc1cncc(NC(=O)OC(C)(C)C)c1
HCID57962286

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1cncc(C#Cc2cc([N+](=O)[O-])ccc2NC(=O)OC(C)(C)C)c1
HCID57961805

未命名化合物

收率 85%

PROCEDURE

实验过程

This compound was prepared according to the procedure of Example B19 step C, using tert-butyl (5-ethynylpyridin-3-yl)carbamate and tert-butyl (2-iodo-4-nitrophenyl)carbamate as the starting material in 85% yield. LCMS calculated for C23H27N4O6(M+H)+: m/z=455.1.

WORKUP

后处理

  1. customThis compound was prepared